Lecture "NMR Spectroscopy in Chemistry, Materials and Life Sciences "
Prof. Dr. Eike Brunner
Tel.: 32631
Neubau Chemische Institute, Raum 236
Thursday, 4. DS (1 p.m.) weekly and Friday, 2. DS (9.20 a.m.) weekly (Fr. alternating lecture and seminar/excercise)
Room: CHE/201
Start date: Friday, October 13, 2023
Exam: Monday, March 4th, 2024, 9:20-10:50, room will be announced later
This lecture (3 SWS) + seminar/excercise (1 SWS) for Master students (Chemistry Master) and PhD students is also eligible for students of other faculties, e.g., from the School of Science.
This lecture teaches the fundamantal principles of NMR spectroscopy as well as its applications for molecular structure determination in chemistry, materials and life sciences.
Main topics:
- "classical" vector model, Bloch equations and relaxation
- product operator formalism
- RF pulses and pulse sequences
- 1D and 2D Fourier transform NMR spectroscopy
- magnetic interactions (chemical shift, J coupling, magnetic dipole-dipole interaction, electric quadrupole interaction)
- nuclear Overhauser effect (NOE)
- molecular structure determination especially by liquid-state NMR spectroscopy
- basic principles of solid-state NMR spectroscopy
Examination: Written, February 22, 2023, 10:30 a.m., CHE/201
Literature:
- Y. Ning "Structural Identification of Organic Compounds with Spectroscopic Techniques", Wiley-VCH 2005
- J. Cavanagh, W.J. Fairbrother, A.G. Palmer III, N.J. Skelton "Protein NMR Spectroscopy", Academic Press 1996
- R. Ernst, G. Bodenhausen, A. Wokaun "Principles of Nuclear Magnetic Resonance in One and Two Dimensions ", Oxford University Press 1990
- Horst Friebolin "Basic One- and Two-Dimensional NMR Spectroscopy", Wiley-VCH, 5th Edition, 2011
Exercises you can find here: Bildungsportal Sachsen (Enrollment required)
Enrollment: via Bildungsportal Sachsen.