Lecture "NMR Spectroscopy in Chemistry, Materials and Life Sciences "

Prof. Dr. Eike Brunner
Tel.: 32631
Neubau Chemische Institute, Raum 236

© Kolbe et al., Discov Mater 1 (2021) 3

Thursday, 4. DS (1 p.m.) weekly, room CHE/089/H
Friday, 2. DS (9.20 a.m.) weekly (alternating lecture and seminar/excercise), room CHE/S91

Start date: Thursday, October 17, 2024, 4. DS (1:00 p.m.)

Exam: Thursday, February 27^th, 2025, 9:20 a.m.

This lecture (3 SWS) + seminar/excercise (1 SWS) for Master students (Chemistry Master) and PhD students is also eligible for students of other faculties, e.g., from the School of Science. 

Important notice for students not enrolled in the Master course (e.g., PhD students, others) needing a certificate of attendance:
If you need a certificate of attendance for this lecture, it is your duty to contact me at the beginnning of the semester (ideally in the first lecture) and inform me about your attendance! 

This lecture teaches the fundamantal principles of NMR spectroscopy as well as its applications for molecular structure determination in chemistry, materials and life sciences.

Main topics:

• "classical" vector model, Bloch equations and relaxation
• product operator formalism
• RF pulses and pulse sequences
• 1D and 2D Fourier transform NMR spectroscopy
• magnetic interactions (chemical shift, J coupling, magnetic dipole-dipole interaction, electric quadrupole interaction)
• nuclear Overhauser effect (NOE)
• molecular structure determination especially by liquid-state NMR spectroscopy
• basic principles of solid-state NMR spectroscopy

Examination:  Written, February 22, 2023,  10:30 a.m., CHE/201

Literature:

• Y. Ning "Structural Identification of Organic Compounds with Spectroscopic Techniques", Wiley-VCH 2005
• J. Cavanagh, W.J. Fairbrother, A.G. Palmer III, N.J. Skelton "Protein NMR Spectroscopy", Academic Press 1996
• R. Ernst, G. Bodenhausen, A. Wokaun "Principles of Nuclear Magnetic Resonance in One and Two Dimensions ", Oxford University Press 1990
• Horst Friebolin "Basic One- and Two-Dimensional NMR Spectroscopy", Wiley-VCH, 5th Edition, 2011

Exercises you can find here: Bildungsportal Sachsen (Enrollment required) 

Enrollment: via Bildungsportal Sachsen.