Equipment for instrumental chemical analyses

The development of new materials and products as part of industrial research is based on analytics ensuring process reliability and quality control. In our laboratory, all types of textile materials can be characterized in terms of surface and interface properties. Furthermore, thermal properties as well as corresponding changes of state can be determined for polymer materials. Our equipment includes a scanning electron microscope QUANTA FEG 250 in addition to the functionalization and measurement methods listed below. 

Instrumentelle Analytik © ITM/TUD
Atomic absorption spectrometer ZEEnit 700
Atomabsorptionsspektrometer © ITM/TUD

Atomic absorption spectrometer ZEEnit 700

Technical data Features
  • Manufacturer: Analytic Jena
  • Flame, graphite furnace
  • Quantitative determination of metals, metalloids, and some non-metals; partially within ppb range (e.g. Ag: 0,1 μg/l)
Corona pretreatment system ASCS 11-200
Corona Plasmaanlage © ITM/TUD

Corona pretreatment system ASCS 11-200

Technical data Features
  • Manufacturer: Ahlbrandt System GmbH
  • 1200 W - 4000 W
  • Working width 1 m
  • Speeds of up to 4 m/min, self-propelled
  • Planar treatment in continuous operation for the pretreatment and surface activation of textiles and films
  • Operation based on various process gases
  • Precursor supply: liquid or dispersed in gas phase
  • Yarns can be treated individually
Dynamic differential calorimetry DSC Q2000
Differenzkalorimetrie © ITM/TUD

Dynamic differential calorimetry DSC Q2000

Technical Data Features
  • Manufacturer: TA Instruments




 
  • Measurements of heat flows in materials depending on temperature and time under controlled atmosphere
  • Determination of material properties, e.g. glass transition, melting point, crystallisation temperature/time/degree, purity, reaction heat, stabilities, curing degree/temperature, further thermally induced phase transitions
Infrared spectroscopy FT-IR Nicolet 6700
Infrarotspektrometer © ITM/TUD

Infrared spectroscopy FT-IR Nicolet 6700

Technical data Features
  • Manufacturer: Thermo Scientific
  • ATR unit (attenuated total reflexion) with germanium and diamond crystal
  • Spectral range 4000 - 650 cm-1
  • Resolution up to 0,25 cm-1
  • Implementation of infrared spectroscopic examinations for qualitative structural elucidation and for quantification of chemical properties
  • Various clamp heads for two-dimensional, powdery, or extremely hard materials
  • Integrated ATR sample unit
  • Analysis technology for the characterization of manufactured tailored carbon fibers within the „Research Center Carbon Fibers Saxony (RCCF)”
Karl Fischer Titrator, TitroLine 7500 KF
Titrator © ITM/TUD

Karl Fischer Titrator, TitroLine 7500 KF

Technical data Features
  • Manufacturer: SI Analytics
  • Volumetric determination of water in organic solvents and solutions
Climatic test chamber type DY110
Das Foto zeigt einen Klimaprüfschrank mit geöffneter Tür. © ITM/TUD

Climatic test chamber type DY110

Technical data Special features
  • Manufacturer: ATT Umweltsimulation GmbH
  • Temperature range: -40°C to +180°C
  • Temperature change rates:

    Heating: 3.2 K/min

    Cooling: 4.0 K/min
  • Humidity range: 10% rel. F. to 95% rel. F.
  • Temperature range during climate operation: +10°C to +95°C
  • Dimensions of testing chamber: 548 x 447 x 447 mm
  • Integration of UV lamp for exposure trials
  • Manual as well as automated climate operation with temperautre ramps; can be controlled and programmed via external software
  • Recording of temperature and humidity curves during testing and reading via USB interface
  • Integration of, e.g., external measuring technology via sealable opening in climate chamber
Contact angle measuring system DSA 100
Kontaktwinkelmessgerät © ITM/TUD

Contact angle measuring system DSA 100

Heizkammer © ITM/TUD

Heating chamber

Foto auf dem das Prüfgerät DSA100 mit Heizkammer zu sehen ist © ITM/TUD

DSA 100 with integrated heating chamber

Technical data Features
  • Manufacturer: Krüss
  • Measuring statistical and dynamic contact angles of liquids with varying polarity on textile surfaces, foils, and solids (at temperatures of up to 400 °C)
  • Characterization of wetting properties
  • Determination of interface tension of liquid systems
  • Determination of surface energies regarding dispers and polar fractions and differentiation of acid and alkaline functions
  • Analysis technology for the characterization of manufactured tailored carbon fibers within the „Research Center Carbon Fibers Saxony (RCCF)”
Optical microscope
Lichtmikroskop © ITM/TUD

Optical microscope

Technical data Features
  • Manufacturer: Zeiss
  • Reflected light and transmitted light microscopy
  • Polarization for reflected light and transmitted light microscopy
Relyon plasma generator PG-31
Plasmafackel © ITM/TUD

Relyon plasma generator PG-31

Technical data Features
  • Manufacturer: Relyon plasma
  • 700 W - 1000 W
  • Various nozzle geometries
  • 40 kHz - 65 kHz
Rheometer Haake RheoWin /Thermo Scientific Mars II
Rheometer Haake © ITM/TUD

7) Rheometer Haake RheoWin /Thermo Scientific Mars II

Technical data Features
  • Manufacturer: Thermo Scientific
  • Plate/ plate and cone / plate measurement geometry
  • Investigation of the rheology of solutions, dispersions, and melts (flow and viscosity curves)
Tensiometer K100
Tensiometer K100 © ITM/TUD

Single fiber tensiometer SF 100

Technical data Features
  • Manufacturer: Krüss
  • Measurement of contact angles of single fibres (minimum 6 μm)
  • Determination of surface energy and its differentiation
  • Measurement of liquids/coating formulations (including tempered) to determine their interface properties and to predict their wetting behaviour
  • Characterization of liquid/solid systems to examine compatibility
  • Determination according to Wilhelmy
  • Wetting measurements of fiber bundles and powders by means of the Washburn method
  • Analysis technology for the characterization of manufactured tailored carbon fibers within the „Research Center Carbon Fibers Saxony (RCCF)”
Thermogravimetry TGA Q500
Thermogravimetrie © ITM/TUD

Thermogravimetry TGA Q500

Technical data Features
  • Manufacturer: TA Instruments
  • Investigation of physical/chemical processes and reactions in materials related to mass changes
  • Recording of pyrolytic, oxidative, and degradative processes at temperatures ranging up to 1000 °C
UV-Vis-Spectrometer Specord 50 plus
UV-VIS-Spektrometer © ITM/TUD

UV-Vis-Spectrometer Specord 50 plus

Technical data Features
  • Manufacturer: Analytik Jena
  • Single beam photometer
  • Spectral measurement range 190 - 1100 nm
  • Spectral increments up to 0.02 nm
  • Absorption range -3A - 3A
  • Transmission meaurement of liquids and solids
  • Analysis of liquid and solid materials in the UV-VIS range
  • Colorimetry unit for the determination of color shades, depths, and differences in the CIE L*a*b* coordinate system in addition to the degree of whiteness
  • Investigation of solutions and films/solids
  • Large specimen compartment for universal add-ons/equipment
  • 75 mm integrating sphere for reflexion and diffusion measurements  of solids and powders
  • Evaluation of results in terms of colorimetry
Xeno test device: Q-SUN Xe-2 xenon text chamber
Xenotester © ITM/TUD

Xeno test device: Q-SUN Xe-2 xenon text chamber

Technical data Features
  • Manufacturer: Q LAB
  • Weathering, light fastness, and photo stability tests

Moreover, state-of-the-art nanoanalytical equipment is available at one of TUD´s central facilities called Dresden Center for Nanoanalysis (DCN), including transmission electron microscopes, X-ray microscropes, and acoustic atomic force microscopes.

Employee at the ITM © Mirko Krziwon
Name

Ms Dipl.-Ing. Irina Kuznik

Research Group Leader Textile Chemistry & Finishing

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Breitscheidstraße 78, House D, Room 1.1.02

01237 Dresden

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Last modified: Apr 11, 2024